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About

About

I graduated in Applied Physics (Optics and Lasers) at the University of Minho (1996), obtained the MSc in Optoelectronics and Lasers at the Physics Department of the University of Porto (2000); in 2006 I concluded a PhD program at Porto University in collaboration with the Department of Physics and Optical Sciences at the University of North Carolina at Charlotte, NC, USA, with work in luminescence based optical fibre systems for biochemical sensing applications using quantum dots. Since 1997 I have been involved in several research and technology transfer projects related to optical fibre sensing technology, developing new sensing configurations and interrogation techniques for optical sensors. I am, since 2007 a Senior researcher at INESC TEC reponsible for the Biochemical Sensors team, where we explore the potential of optical fibre and integrated optics technologies in environmental and medical applications framed by several R&D projects. I have more than 200 publications in the fields of sensors in national and international conferences and peer reviewed journals, I am author of 3 book chapters and also hold one patent. I am a member of SPIE and SPOF.

Interest
Topics
Details

Details

  • Nationality

    Portugal
  • Centre

    Applied Photonics
  • Contacts

    +351220402301
    pedro.jorge@inesctec.pt
028
Publications

2023

Intelligent grids for faster elemental mapping with Laser-induced breakdown spectroscopy

Authors
Capela, D; Ferreira, M; Lima, A; Jorge, P; Guimarães, D; Silva, NA;

Publication
Results in Optics

Abstract
Laser-induced breakdown spectroscopy is a spectroscopic technique that allows for fast elemental mapping of heterogeneous samples. Yet, detailed maps need high-resolution sampling grids, which can turn the task into a time-consuming process and can increase sample damage. In this work, we present the implementation of an imaged-based intelligent mesh algorithm that makes use of superpixel segmentation to optimize elemental mapping processes. Our results show that the approach can increase the elemental mapping resolution and decrease acquisition times, fostering opportunities for applications that benefit from minimal sample damage such as heritage analysis, or timely analysis such as industrial applications. © 2022 The Author(s)

2023

Compact biosensor system for the quantification of hydrogen peroxide in milk

Authors
Vasconcelos, H; Matias, A; Mendes, J; Araujo, J; Dias, B; Jorge, PAS; Saraiva, C; de Almeida, JMMM; Coelho, LCC;

Publication
TALANTA

Abstract
Hydrogen peroxide is usually added to products to delay the development of microorganisms mainly in milk, hence increasing its stability over time, however the side effects can become devastating to human health.A technique is presented consisting of detecting hydrogen peroxide as an adulterant in milk through a sensor where pretreatment of the sample is not necessary, using a single use membrane. The detection of hydrogen peroxide in fresh-raw, whole, semi-skimmed and skimmed milk was performed using a luminol chem-iluminescence reaction.For hydrogen peroxide water solutions, a linear response was attained from 1.0 x 10-4 to 9.0 x 10-3 %w/w and an LOD (limit of detection) of 3.0 x 10-5 %w/w was determined. An R-squared value of 0.97 and a relative standard deviation lower than 10%, were achieved.Hydrogen peroxide concentration as low as 1.0 x 10-3 %w/w was measured for fresh-raw, skim and whole milk and for semi-skimmed milk, as low as 2.0 x 10-3 %w/w.The methodology presented, as long as our knowledge, is original, rapid, ecological and inexpensive. In regard of the sensitivity obtained, the methodology has great possibility to be applied in the detection of hydrogen peroxide in several areas. It is envisaged monitoring of food quality, agriculture systems and environment pollution.

2023

Interactive three-dimensional chemical element maps with laser-induced breakdown spectroscopy and photogrammetry

Authors
Lopes, T; Rodrigues, P; Cavaco, R; Capela, D; Ferreira, MFS; Guimaraes, D; Jorge, PAS; Silva, NA;

Publication
SPECTROCHIMICA ACTA PART B-ATOMIC SPECTROSCOPY

Abstract
Imaging the spatial distribution of chemical elements at a sample surface is a common application of laserinduced breakdown spectroscopy with vast scientific and technological applications. Yet, typical imaging solutions only explore the creation of two-dimensional maps, which can limit the interpretability of the results and further diagnostics in three-dimensional settings. Within this context, this work explores the combination of spectral imaging techniques and photogrammetry to deploy a versatile solution for the creation of threedimensional spectral imaging models. First, by making use of a numerical algorithm that is able to match features in the spectral image with those of the three-dimensional model, we show how to match the mesh from distinct sensor modalities. Then, we describe a possible visualization workflow, making use of dedicated photogrammetry and visualization software to easily deploy interactive models. Overall, the results demonstrate the versatility of our approach and pave for the development of novel spectral imaging diagnostic strategies that are able to deliver better qualitative analysis and insight in the three-dimensional space.

2023

Imprinted Hydrogel Nanoparticles for Protein Biosensing: A Review

Authors
Silva, AT; Figueiredo, R; Azenha, M; Jorge, PAS; Pereira, CM; Ribeiro, JA;

Publication
ACS SENSORS

Abstract
Over the past decade, molecular imprinting (MI) technologyhasmade tremendous progress, and the advancements in nanotechnology havebeen the major driving force behind the improvement of MI technology.The preparation of nanoscale imprinted materials, i.e., molecularlyimprinted polymer nanoparticles (MIP NPs, also commonly called nanoMIPs),opened new horizons in terms of practical applications, includingin the field of sensors. Currently, hydrogels are very promising forapplications in bioanalytical assays and sensors due to their highbiocompatibility and possibility to tune chemical composition, size(microgels, nanogels, etc.), and format (nanostructures, MIP film,fibers, etc.) to prepare optimized analyte-responsive imprinted materials.This review aims to highlight the recent progress on the use of hydrogelMIP NPs for biosensing purposes over the past decade, mainly focusingon their incorporation on sensing devices for detection of a fundamentalclass of biomolecules, the peptides and proteins. The review beginsby directing its focus on the ability of MIPs to replace biologicalantibodies in (bio)analytical assays and highlight their great potentialto face the current demands of chemical sensing in several fields,such as disease diagnosis, food safety, environmental monitoring,among others. After that, we address the general advantages of nanosizedMIPs over macro/micro-MIP materials, such as higher affinity towardtarget analytes and improved binding kinetics. Then, we provide ageneral overview on hydrogel properties and their great advantagesfor applications in the field of Sensors, followed by a brief descriptionon current popular routes for synthesis of imprinted hydrogel nanospherestargeting large biomolecules, namely precipitation polymerizationand solid-phase synthesis, along with fruitful combination with epitopeimprinting as reliable approaches for developing optimized protein-imprintedmaterials. In the second part of the review, we have provided thestate of the art on the application of MIP nanogels for screeningmacromolecules with sensors having different transduction modes (optical,electrochemical, thermal, etc.) and design formats for single use,reusable, continuous monitoring, and even multiple analyte detectionin specialized laboratories or in situ using mobiletechnology. Finally, we explore aspects about the development of thistechnology and its applications and discuss areas of future growth.

2023

Conditioning Solid-State Anode-Less Cells for the Next Generation of Batteries

Authors
Baptista, MC; Gomes, BM; Capela, D; Ferreira, MFS; Guimaraes, D; Silva, NA; Jorge, PAS; Silva, JJ; Braga, MH;

Publication
BATTERIES-BASEL

Abstract
Anode-less batteries are a promising innovation in energy storage technology, eliminating the need for traditional anodes and offering potential improvements in efficiency and capacity. Here, we have fabricated and tested two types of anode-less pouch cells, the first using solely a copper negative current collector and the other the same current collector but coated with a nucleation seed ZnO layer. Both types of cells used the same all-solid-state electrolyte, Li2.99Ba0.005ClO composite, in a cellulose matrix and a LiFePO4 cathode. Direct and indirect methods confirmed Li metal anode plating after charging the cells. The direct methods are X-ray photoelectron spectroscopy (XPS) and laser-induced breakdown spectroscopy (LIBS), a technique not divulged in the battery world but friendly to study the surface of the negative current collector, as it detects lithium. The indirect methods used were electrochemical cycling and impedance and scanning electron microscopy (SEM). It became evident the presence of plated Li on the surface of the current collector in contact with the electrolyte upon charging, both directly and indirectly. A maximum average lithium plating thickness of 2.9 mu m was charged, and 0.13 mu m was discharged. The discharge initiates from a maximum potential of 3.2 V, solely possible if an anode-like high chemical potential phase, such as Li, would form while plating. Although the ratings and energy densities are minor in this study, it was concluded that a layer of ZnO, even at 25 degrees C, allows for higher discharge power for more hours than plain Cu. It was observed that where Li plates on ZnO, Zn is not detected or barely detected by XPS. The present anode-less cells discharge quickly initially at higher potentials but may hold a discharge potential for many hours, likely due to the ferroelectric character of the electrolyte.

Supervised
thesis

2022

Sensores ópticos para medição de campos magnéticos baseados em ondas eletromagnéticas de superfície

Author
João Pedro Miranda Carvalho

Institution
UP-FCUP

2022

Development of optical Sensors for Carbon Dioxide Detection

Author
Nuno Alexandre Pereira Mendes

Institution
UP-FEUP

2022

Fabrication of opticals Ensing devices by 3D laser  micromachining

Author
Carlos Duarte Rodrigues Viveiros

Institution
UP-FCUP

2022

Towards Realtime Classification of Optically Trapped Particles

Author
Vicente Vieira Rocha

Institution
UP-FCUP

2022

Development of differential optrodes for highly sensitive and reliable chemical sensing

Author
João Pedro Sampaio Mendes

Institution
UP-FCUP