2017
Authors
Fleming, DEB; Nader, MN; Foran, KA; Groskopf, C; Reno, MC; Ware, CS; Tehrani, M; Guimaraes, D; Parsons, PJ;
Publication
APPLIED RADIATION AND ISOTOPES
Abstract
The feasibility of measuring arsenic and selenium contents in a single nail clipping was investigated using a small-focus portable X-ray fluorescence (XRF) instrument with monochromatic excitation beams. Nail clipping phantoms supplemented with arsenic and selenium to produce materials with 0, 5, 10, 15, and 20 mu g/g were used for calibration purposes. In total, 10 different clippings were analyzed at two different measurement positions. Energy spectra were fit with detection peaks for arsenic K-alpha, selenium K-alpha, arsenic K-beta, selenium K-beta, and bromine K-alpha characteristic X-rays. Data analysis was performed under two distinct conditions of fitting constraint. Calibration lines were established from the amplitude of each of the arsenic and selenium peaks as a function of the elemental contents in the clippings. The slopes of the four calibration lines were consistent between the two conditions of analysis. The calculated minimum detection limit (MDL) of the method, when considering the Ka peak only, ranged from 0.210 +/- 0.002 mu g/g selenium under one condition of analysis to 0.777 +/- 0.009 mu g/g selenium under another. Compared with previous portable XRF nail clipping studies, MDLs were substantially improved for both arsenic and selenium. The new measurement technique had the additional benefits of being short in duration (similar to 3 min) and requiring only a single nail clipping. The mass of the individual clipping used did not appear to play a major role in signal strength, but positioning of the clipping is important.
2017
Authors
Novais, S; Ferreira, MS; Pinto, JL;
Publication
THIRD INTERNATIONAL CONFERENCE ON APPLICATIONS OF OPTICS AND PHOTONICS
Abstract
A Fabry-Perot air bubble microcavity fabricated between a section of single mode fiber and a multimode fiber is proposed. The study of the microcavities growth with the number of applied arcs is performed. The sensors are tested for lateral load and strain, where sensitivities of 0.32 nm/N and 2.11 nm/N and of 4.49 pm/mu epsilon and 9.12 pm/mu epsilon are obtained for the 47 mu m and 161 mu m long cavities, respectively. The way of manufacturing using a standard fusion splicer and given that no oils or etching solutions are involved, emerges as an alternative to the previously developed air bubble based sensors.
2017
Authors
Novais, S; Ferreira, MS; Pinto, JL;
Publication
IEEE PHOTONICS TECHNOLOGY LETTERS
Abstract
A Fabry-Perot air bubble microcavity fabricated between a section of single mode fiber and a multimode fiber that requires only the use of a commercial fusion splicer is proposed. The study of the microcavities growth with the number of applied arcs is performed and several sensors are tested. The sensors are tested for lateral load measurements, and it is observed that there is dependence between the sensor dimensions and its sensitivity. The maximum sensitivity of 2.11 nm/N was obtained for the 161-mu m-long cavity. Moreover, given the low temperature sensitivity (<1 pm/degrees C), the proposed cavity should be adequate to perform temperature-independent measurements. The accurate technique control leads to the fabrication of reproducible cavities with the sensitivity required for the application. The way of manufacturing using a standard fusion splicer, given that no oils or etching solutions are involved, emerges as an alternative to the previously developed air bubble-based sensors.
2017
Authors
Franciscangelis, C; Margulis, W; Floridia, C; Rosolem, JB; Salgado, FC; Nyman, T; Petersson, M; Hallander, P; Hällstrom, S; Söderquist, I; Fruett, F;
Publication
SPIE Proceedings - Sensors and Smart Structures Technologies for Civil, Mechanical, and Aerospace Systems 2017
Abstract
2017
Authors
Lima dos Reis Marques, F; Floridia, C; Alves Almeida, T; Leonardi, AA; Fruett, F;
Publication
2017 SBMO/IEEE MTT-S International Microwave and Optoelectronics Conference (IMOC)
Abstract
2017
Authors
Rosolem, JB; Penze, RS; Floridia, C; Dini, DC; Peres, R; do Nascimento, CAM; Valadares, JEF;
Publication
2017 SBMO/IEEE MTT-S International Microwave and Optoelectronics Conference (IMOC)
Abstract
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