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Publications

Publications by Pedro Jorge

2019

Low-Cost Interrogation System for Long-Period Fiber Gratings Applied to Remote Sensing

Authors
dos Santos, PSS; Jorge, PAS; de Almeida, JMMM; Coelho, L;

Publication
SENSORS

Abstract
We present a portable and low-cost system for interrogation of long-period fiber gratings (LPFGs) costing around a 30th of the price of a typical setup using an optical spectrum analyzer and a broadband light source. The unit is capable of performing real-time monitoring or as a stand-alone data-logger. The proposed technique uses three thermally modulated fiber-coupled laser diodes, sweeping a few nanometers around their central wavelength. The light signal is then modulated by the LPFG and its intensity is acquired by a single photo-detector. Through curve-fitting algorithms the sensor transmission spectrum is reconstructed. Testing and validation were accomplished by inducing variations in the spectral features of an LPFG through changes either in external air temperature from 22 to 425 degrees C or in refractive index (RI) of the surrounding medium from 1.3000 to 1.4240. A dynamic resolution between 3.5 and 1.9 degrees C was achieved, in temperatures from 125 to 325 degrees C. In RI measurements, maximum wavelength and optical power deviations of 2.75 nm and 2.86 dB, respectively, were obtained in the range from 1530 to 1570 nm. The worse RI resolution obtained was 3.47x10(-3). The interrogation platform was then applied in the detection of iron corrosion, expressing wavelength peak values within 1.12 nm from the real value in the region between 1530 and 1570 nm.

2019

Optical Fiber-based Sensing Method for Nanoparticles Detection through Back-Scattering Signal Analysis

Authors
Paiva, JS; Ribeiro, RSR; Jorge, PAS; Rosa, CC; Sampaio, P; Cunha, JPS;

Publication
OPTICAL FIBERS AND SENSORS FOR MEDICAL DIAGNOSTICS AND TREATMENT APPLICATIONS XIX

Abstract
In view of the growing importance of nanotechnologies, the detection of nanoparticles type in several contexts has been considered a relevant topic. Several organisms, including the National Institutes of Health, have been highlighting the urge of developing nanoparticles exposure risk assessment assays, since very little is known about their physiological responses. Although the identi fi cation/characterization of synthetically produced nanoparticles is considered a priority, there are many examples of \ naturally" generated nanostructures that provide useful information about food components or human physiology. In fact, several nanoscale extracellular vesicles are present in physiological fluids with high potential as cancer biomarkers. However, scientists have struggled to fi nd a simple and rapid method to accurately detect/identify nanoparticles, since their majority have diameters between 100-150 nm -far below the di ff raction limit. Currently, there is a lack of instruments for nanoparticles detection and the few instrumentation that is commonly used is costly, bulky, complex and time consuming. Thus, considering our recent studies on particles identi fi cation through back-scattering, we examined if the time/frequency-domain features of the back-scattered signal provided from a 100 nm polystyrene nanoparticles suspension are able to detect their presence only by dipping a polymeric lensed optical fi ber in the solution. This novel technique allowed the detection of synthetic nanoparticles in distilled water versus \ blank solutions" (only distilled water) through Multivariate Statistics and Arti fi cial Intelligence (AI)-based techniques. While the state-of-the-art methods do not o ff er a ff ordable and simple approaches for nanoparticles detection, our technique can contribute for the development of a device with innovative characteristics.

2019

Spectral Tuning of Long Period Fiber Gratings Fabricated by Femtosecond Laser Micromachining through Thermal Annealing

Authors
Viveiros, D; Almeida, JMMMd; Coelho, L; Vasconcelos, H; Amorim, VA; Maia, JM; Jorge, PAS;

Publication
Proceedings

Abstract
A femtosecond laser direct writing system was developed to explore the fabrication of long-period fiber gratings (LPFGs) in SMF28 fibers. The LPFGs, showing the mode LP1,6 at 1500 nm, were exposed to high-temperature annealing up to 950 °C. Modifications in the refractive index (RI) modulation are observed through a blue-shift in the LPFG attenuation bands and above 850 °C, the mode LP1,7 appear at 1600 nm. The wavelength sensitivity to external RI from 1.300 to 1.452 was estimated for both modes before and after annealing. Greater sensitivity was found for the higher order mode in the entire range reaching 2400 nm/RIU around 1.440.

2019

Mach-Zehnder Interferometers Based on Long Period Fiber Grating Coated With Titanium Dioxide for Refractive Index Sensing

Authors
Soares Guedes Vasconcelos, HCASG; Marques Martins de Almeida, JMMM; Teixeira Saraiva, CMT; da Silva Jorge, PAD; Costa Coelho, LCC;

Publication
JOURNAL OF LIGHTWAVE TECHNOLOGY

Abstract
The wavelength sensitivity and spectral resolution of Mach-Zehnder fiber interferometers obtained through a combination of two identical uncoated and titanium dioxide (TiO2) coated long period fiber gratings (LPFGs) is presented and compared with single LPFGs-based refractometric sensors. A set of LPFGs were fabricated in single mode fiber with the resonance band having an amplitude of 3 dB in order to split in half the optical power between the core and the specific cladding modes. The separation between the pair of LPFG written in the fiber was varied between 1 and 3 cm and the thickness of the TiO2 coating around the fiber ranged from 20 to 40 nm. A wavelength shift sensitivity of 216 nm/refractive index units (RIU) was achieved for the device with 3 cm and a 30-nm thick TiO2 coating, which presented a spectral resolution of 1.1 x 10(-4 )Rill Despite the lower wavelength shift sensitivity of 142 nm/RIU, attained for a 2-cm long device and 30-nm thick TiO2 coating, a spectral resolution of 1.8 x 10(-5) RIU was measured, which is one order of magnitude lower than a single LPFG.

2019

Alkali-silica reaction in concrete: Mechanisms, mitigation and test methods

Authors
Figueira, RB; Sousa, R; Coelho, L; Azenha, M; de Almeida, JM; Jorge, PAS; Silva, CJR;

Publication
CONSTRUCTION AND BUILDING MATERIALS

Abstract
In the last few decades, the alkali-silica reaction (ASR) has been reported as one of the major concrete concerns regarding durability, leading to high maintenance and reconstruction costs. The occurrence of ASR in numerous concrete infrastructures all over the world points to the need for research regarding measures for its detection in an initial stage (and further mitigation) either in new or existing structures. Furthermore, the chemical and physical mechanisms for ASR remain poorly understood. This lack of knowledge leads to incapacity to assess risk, cost-effectively predict service life, and efficiently mitigate the deterioration process due to ASR in concrete structures. This manuscript aims to review the most recent and relevant achievements and the existing knowledge concerning the reaction mechanisms of ASR. Additionally, this manuscript is focused on the conditioning factors, diagnostic and prognostic methodologies, preventive measures and test methods (including their limitations) of ASR conducted at an academic level. The perspectives for future research challenges are also identified and debated.

2019

A Novel Method for Scatterers Type Enumeration in Polydisperse Suspensions through Fiber Trapping and Unsupervised Scattering Analysis

Authors
Paiva, JS; Ribeiro, RSR; Jorge, PAS; Rosa, CC; Sampaio, P; Cunha, JPS;

Publication
IMAGING, MANIPULATION, AND ANALYSIS OF BIOMOLECULES, CELLS, AND TISSUES XVII

Abstract
Colloids and suspensions are part of our daily routines. Even the blood is considered a "naturally" occurring colloid. However, the majority of colloids are complex and composed by a diversity of nano to microparticles. The characterization of both synthetic and physiological fluids in terms of particulate types, size and surface characteristics plays a vital role in products formulation, and in the early diagnosis through the identification of abnormal scatterers in physiological fluids, respectively. Several methods have been proposed for characterizing suspensions, including imaging, electrical sensing counters, hydrodynamic or field flow fractionation. However, the Dynamic Light Scattering (DLS) has evolved as the most convenient method from these. Based also on the scattering signal, we propose a novel, simple and fast method able to determine the number of different scatterers type present in a suspension, without any previous information about its composition (in terms of particle classes). This is achieved by collecting features from a 980 nm laser back-scattered signal acquired through a polymeric lensed optical fiber tip dipped into the solution. Unlike DLS, this technique allows the trapping of particles whose diameter >= 1 mu m. For smaller particles, despite not guaranteeing their immobilization, it is also able to determine the number of different nanoparticles classes in an ensemble. The number of particle types was correctly determined for suspensions of synthetic particles and yeasts; different bacteria; and 100 nm nanoparticles types, using both Principal Component Analysis and K-means algorithms. This method could be a valuable alternative to complex and time-consuming methods for particles separation, such as field flow fractionation.

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