2023
Autores
Ferreira, MFS; Guimaraes, D; Oliveira, R; Lopes, T; Capela, D; Marrafa, J; Meneses, P; Oliveira, A; Baptista, C; Gomes, T; Moutinho, S; Coelho, J; da Silva, RN; Silva, NA; Jorge, PAS;
Publicação
SENSORS
Abstract
Evaluating the efficiency of surface treatments is a problem of paramount importance for the cork stopper industry. Generically, these treatments create coatings that aim to enhance the impermeability and lubrification of cork stoppers. Yet, current methods of surface analysis are typically time-consuming, destructive, have poor representativity or rely on indirect approaches. In this work, the use of a laser-induced breakdown spectroscopy (LIBS) imaging solution is explored for evaluating the presence of coating along the cylindrical surface and in depth. To test it, several cork stoppers with different shaped areas of untreated surface were analyzed by LIBS, making a rectangular grid of spots with multiple shots per spot, to try to identify the correspondent shape. Results show that this technique can detect the untreated area along with other features, such as leakage and holes, allowing for a high success rate of identification and for its performance at different depths, paving the way for future industry-grade quality control solutions with more complex surface analysis.
2023
Autores
Carvalho, PM; Coelho, CC; Jorge, PAS; de Almeida, JMMM;
Publicação
Proceedings - 28th International Conference on Optical Fiber Sensors, OFS 2023
Abstract
Thin films of Ag/Fe were deposited on the core of multimode optical fibers. The deposited film shows sensitivity to both refractive index and MF changes. Simulation work based on TMM formalism confirms experimental response. © Optica Publishing Group 2023, © 2023 The Author(s)
2023
Autores
Soares, L; Perez Herrera, RA; Novais, S; Ferreira, A; Silva, S; Frazao, O;
Publicação
PHOTONICS
Abstract
Process Analytical Technology (PAT) has been increasingly used in the pharmaceutical industry to monitor essential parameters in real-time during pharmaceutical processes. The concentration of Active Pharmaceutical Ingredients (APIs), such as paracetamol, is one of these parameters, and controlling its variations allows for optimization of the production process. In this study, a refractometric sensor, implemented by an interrogation system based on an Erbium-Doped Fiber Ring Cavity (EDFRC), was presented and experimentally demonstrated. The Cavity Ring proposed included a 1 x 3 coupler. One port of the coupler was used to increase the optical power of the system through a Fiber Bragg Grating (FBG), and the other two ports were used as sensing head and reference. The sensor detected variations of paracetamol concentration with a sensitivity of [(-1.00 +/- 0.05) x 10(-3)] nW/(g/kg) and a resolution of 5.53 g/kg. The results demonstrate the potential of this technology as a possible non-invasive PAT tool.
2023
Autores
Robalinho, P; Soares, B; Lobo, A; Silva, S; Frazao, O;
Publicação
SENSORS
Abstract
In this paper, a different Fiber Loop Mirror (FLM) configuration with two circulators is presented. This configuration is demonstrated and characterized for sensing applications. This new design concept was used for strain and torsion discrimination. For strain measurement, the interference fringe displacement has a sensitivity of (0.576 +/- 0.009) pm.mu epsilon(-1). When the FFT (Fast Fourier Transformer) is calculated and the frequency shift and signal amplitude are monitored, the sensitivities are (-2.1 +/- 0.3) x 10(-4) nm(-1) mu epsilon(-1) and (4.9 +/- 0.3) x 10(-7) mu epsilon(-1), respectively. For the characterization in torsion, an FFT peaks variation of (-2.177 +/- 0.002) x 10(-12) nm(-1)/degrees and an amplitude variation of (1.02 +/- 0.06) x 10(-3)/degrees are achieved. This configuration allows the use of a wide range of fiber lengths and with different refractive indices for controlling the free spectral range (FSR) and achieving refractive index differences, i.e., birefringence, higher than 10(-2), which is essential for the development of high sensitivity physical parameter sensors, such as operating on the Vernier effect. Furthermore, this FLM configuration allows the system to be balanced, which is not possible with traditional FLMs.
2023
Autores
Soares, L; Perez-Herrera, RA; Novais, S; Ferreira, A; Frazao, O; Silva, S;
Publicação
2023 IEEE 7TH PORTUGUESE MEETING ON BIOENGINEERING, ENBENG
Abstract
A linear fiber laser system for measurements of paracetamol concentration is experimentally demonstrated. The cavity is based on a fiber loop mirror and an FBG centered at 1567.8 nm. The sensing head corresponds to a refractometric sensor, whose which principle of operation is based on Fresnel reflection in the fiber tip (FBG side). The system works at detected variations of paracetamol concentrations with a sensitivity of [(8.74 +/- 0.34) x10(-5)] mu W/(g/kg) and a resolution of 2.77 g/kg. The results prove that the fiber laser system could be an asset for processing industries, specifically for non-invasive and real-time measurements of concentration.
2023
Autores
Cunha, C; Assuncao, AS; Monteiro, CS; Leitao, C; Mendes, JP; Silva, S; Frazao, O; Novais, S;
Publicação
2023 IEEE 7TH PORTUGUESE MEETING ON BIOENGINEERING, ENBENG
Abstract
Using surface resonance (SPR) as a sensitivity enhancer, this work describes the development of a transmissive multimode optical fiber sensor with a gold (Au) thin film that measures glucose concentration. The fiber's cladding was initially removed, and an Au layer was then sputtered onto its surface to simultaneously excite SPR and reflect light, making the SPR sensor extremely sensitive to changes in the environment's refractive index. A range of glucose concentrations, from 0.0001 to 0.5000 g/ml, were tested on the sensor. A maximum sensitivity of 161.302 nm/(g/mL) was attained for the lowest glucose concentration, while the highest concentration yielded a sensitivity of 312.000 nm/(g/mL). The proposed sensor's compact size, high sensitivity, good stability and practicality make it a promising candidate for a range of applications, including detecting diabetes.
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