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Publications

Publications by José Almeida

2016

Optical sensor based on hybrid FBG/titanium dioxide coated LPFG for monitoring organic solvents in edible oils

Authors
Coelho, L; Viegas, D; Santos, JL; de Almeida, JMMM;

Publication
TALANTA

Abstract
A hybrid optical sensing scheme based on a fiber Bragg grating (FBG) combined with a titanium dioxide coated long period fiber grating (LPFG) for monitoring organic solvents in high refractive index edible oils is reported. In order to investigate and optimize the sensor performance, two different FBG/LPFG interrogation systems were investigated. The readout of the sensor was implemented using either the wavelength shift of the LPFG resonance dip or the variation in the optical power level of the reflected/transmitted light at the FBG wavelength peak, which in turn depends on the wavelength position of the LPFG resonance. Hexane concentrations up to 20%V/V, corresponding to the refractive index range from 1.451 to 1.467, were considered. For the transmission mode of operation, sensitivities of 1.41 nm/%V/V and 0.11 dB/%V/V, with resolutions of 0.58%V/V and 0.29%V/V, were achieved when using the LPFG wavelength shift and the FBG transmitted optical power, respectively. For the FBG reflection mode of operation, a sensitivity of 0.07 dB/V/V and a resolution better than 0.16%V/V were estimated.

2014

Enhanced refractive index sensing characteristics of optical fibre long period grating coated with titanium dioxide thin films

Authors
Coelho, L; Viegas, D; Santos, JL; de Almeida, JMMM;

Publication
SENSORS AND ACTUATORS B-CHEMICAL

Abstract
A new type of fibre-optic refractive index sensor based on a long period fibre grating (LPFG) coated with a titanium dioxide (TiO2) thin film was demonstrated. The wavelength shift of the attenuation bands of this LPFG sensor to changes in the refractive index of the external media from 1.30 to 1.64 RIU was investigated. In order to optimize the sensor the TiO2 thin film thickness deposited around the LPFGs was varied from 10 to 80 nm. It was found that the TiO2 thin film increases the wavelength sensitivity of the LPFG to changes in the surrounding refractive index for values lower and higher than the cladding refractive index. As opposed to the bare LPFG it was shown the possibility to monitor refractive indices lower and higher than cladding refractive index tailoring the TiO2 thickness. An average wavelength sensitivity of 5250 nm/RIU was achieved in the range 1.444 to 1.456 RIU for a TiO2 thickness of 50 nm. In the region between 1.46 and 1.48 RIU the average sensitivity of about 825 nm/RIU was measured for a 40 nm thick film.

2013

H-2 Sensing Based on a Pd-Coated Tapered-FBG Fabricated by DUV Femtosecond Laser Technique

Authors
Silva, S; Coelho, L; Almeida, JM; Frazao, O; Santos, JL; Malcata, FX; Becker, M; Rothhardt, M; Bartelt, H;

Publication
IEEE PHOTONICS TECHNOLOGY LETTERS

Abstract
An optical fiber probe sensor based on a tapered-fiber Bragg grating (FBG) coated with 150-nm-thick Pd film is proposed for hydrogen detection. The FBG was written in a 50-mu m-diameter tapered fiber by deep ultraviolet femtosecond laser technology. A second FBG was inscribed in the 125 mu m-fiber section for temperature compensation. The sensing head was able to detect H-2 concentration in the range 0%-1% (v/v) H-2 at room temperature; a maximum sensitivity of 81.8 pm/%(v/v) H-2 was attained with temperature compensation. The influence of the Pd coating over temperature sensitivity of standard and tapered-FBGs is also presented.

2017

Monitoring of oxidation phases of copper thin films using long period fiber gratings

Authors
Coelho, L; Agostinho Moreira, JA; Tavares, PB; Santos, JL; Viegas, D; de Almeida, JMMM;

Publication
SENSORS AND ACTUATORS A-PHYSICAL

Abstract
Long period fiber gratings (LPFGs) were used to monitor the characteristics of copper (Cu) thin films when annealed in air atmosphere up to similar to 680 degrees C. The wavelength and the optical power shift of the resonant bands of the LPFGs when coated with the Cu thin films, were measured as a function of the annealing temperature, and were found to exhibit a different evolution comparing to a bare LPFGs. Thin films of Cu deposited on quartz (SiO2) substrates were annealed and analyzed by XRD, SEM/EDS and Raman spectroscopy, allowing to identify the formation of two distinct oxide phases at different temperatures, cuprous (Cu2O-cuprite) and cupric (CuO-tenorite) oxides, respectively. The observed features of the resonant bands of the LPFGs were found to be associated with the Cu oxide phase transitions, indicating the possibility of using LPFGs to monitor, in real time, the oxidation states of Cu thin films by following specific characteristics of the attenuation bands. In addition, LPFGs over coated with the two distinct oxidation phases of Cu were characterized for refractive index sensing in the range between 1.300 to 1.600, leading to the conclusion that the sensitivity to the refractive index of the surrounding medium of Cu coated LPFGs sensing systems can be temperature tuned.

2014

Secondary Ion Mass Spectrometry Study of Erbium Titanium Codiffusion in Lithium Niobate

Authors
de Almeida, JMMM; Marinho, F; Alexandre, D; Sada, C;

Publication
IEEE PHOTONICS TECHNOLOGY LETTERS

Abstract
A study on the influence of titanium on the diffusion kinetics of erbium in lithium niobate is presented. An empirical linear relation between the diffusion coefficient of erbium and the initial film thickness of titanium was obtained from secondary ion mass spectrometry data. An improvement in the diffusion coefficient by a factor of two was measured for a 200-nm titanium film. Furthermore, the erbium and titanium codiffusion process not only enhances the diffusion of erbium, leading to smaller diffusion time, but also improves the device visibility for further fabrication procedures. This letter is envisioned to clarify in a quantitative way the process of simultaneous codiffusion of erbium and titanium ions into lithium niobate, which has been studied by several authors; nevertheless, no definitive conclusion can be found in the literature.

2015

Fiber optic hydrogen sensor based on an etched Bragg grating coated with palladium

Authors
Coelho, L; de Almeida, JMMM; Santos, JL; Viegas, D;

Publication
APPLIED OPTICS

Abstract
A study of a sensor for hydrogen (H-2) detection based on fiber Bragg gratings coated with palladium (Pd) with self-temperature compensation is presented. The cladding around the gratings was reduced down to 50 mu m diameter by a chemical etching process. One of the gratings was left uncoated, and the other was coated with 150 nm of Pd. It was observed that palladium hydride has unstable behavior in environments with high humidity level. A simple solution to overcome this problem based on a Teflon tape is presented. The sensing device studied was able to respond to H-2 concentrations in the range 0%-1% v/v at room temperature and atmospheric pressure, achieving sensitivities larger than 20 pm/% v/v. Considering H-2 concentrations in nitrogen up to 1%, the performance of the sensing head was characterized for different thicknesses of Pd coating ranging from 50 to 200 nm. (C) 2015 Optical Society of America

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